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5. Tetraalkylammonium trifluoromethanesulfonates [3] Et4N(CF3SO3): Add 5 g of CF3SO3H (33 mmol) to 50 g of 10% Et4NOH (34 mmol), stir it for 30 min, and dry it using a rotating evaporator to get crude Et4N(CF3SO3). Recrystallize it three times from THF and dry in a vacuum. An alternative procedure is to recrystallize the crude product from acetone ethyl ether (1:9) and to dry it for 24 h at 60 8C in a vacuum and in the presence of P2O5, mp 160 161 8C. Bu4N(CF3SO3): Dissolve 9.7 g of Bu4NBr (30 mmol) in 30 ml of water, and, with vigorous stirring, slowly add to it 4.5 g of CF3SO3H (30 mmol). After cooling to room temperature, filter the mixture and wash the precipitate with water. Recover the product remaining in the filtrate by extracting with dichloromethane and add it to the above precipitate. Recrystallize the precipitate twice from dichloromethane ether and dry in a vacuum, mp 111 112.5 8C. As an alternative, the method to neutralize Bu4NOH with CF3SO3H can be employed [18]. 6. Other tetraalkylammonium salts Other tetraalkylammonium salts are also used in electrochemical measurements; they are tetraalkylammonium nitrates, picrates, carboxylates, sulfonates, etc. They can be prepared in the laboratory, by neutralizing the corresponding acid in water with R4NOH just to the equivalence point, removing water, and then drying. If necessary, the products are recrystallized. Some tetraalkylammonium salts form hydrates and are difficult completely to dehydrate. For practical information, see, for example, Ref. [19].

19 Chiang Y, Goodrich MT, Grove EF, Tamassia R, Vengroff DE, Vitter JS External-memory graph algorithms Proceedings of the 6th Annual ACM-SIAM Symposium on Discrete Algorithms (SODA 95); 1995 p 139 149 20 Coppersmith D, Kumar R An improved data stream algorithm for frequency moments Proceedings of the 15th Annual ACM-SIAM Symposium on Discrete Algorithms (SODA 04); 2004 p 151 156 21 Cormode G, Muthukrishnan S Estimating dominance norms on multiple data streams Proceedings of the 11th Annual European Symposium on Algorithms (ESA 03); 2003 p 148 160 22 Cormode G, Muthukrishnan S What is hot and what is not: Tracking most frequent items dynamically Proceedings of the 22nd ACM Symposium on Principles of Database Systems (PODS 03); 2003 23 Cormode G, Muthukrishnan S An improved data stream summary: the count-min sketch and its applications J Algorithms 2005;55(1):58 75 24 Cormode G, Muthukrishnan S.

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Space ef cient mining of multigraph streams Proceedings of the 24th ACM Symposium on Principles of Database Systems (PODS 05); 2005 25 Demetrescu C, Finocchi I, Ribichini A Trading off space for passes in graph streaming problems Proceedings of the 17th Annual ACM-SIAM Symposium on Discrete Algorithms (SODA 06); 2006 p 714 723 26 Elkin M, Zhang J Ef cient algorithms for constructing (1 + , )-spanners in the distributed and streaming models Proceedings of the 23rd Annual ACM Symposium on Principles of Distributed Computing (PODC 04); 2004 p 160 168 27 Feigenbaum J, Kannan S, McGregor A, Suri S, Zhang J On graph problems in a semistreaming model Proceedings of the 31st International Colloquium on Automata, Languages and Programming (ICALP 04); 2004 28 Feigenbaum J, Kannan S, McGregor A, Suri S, Zhang J Graph distances in the streaming model: the value of space.

As discussed in the previous chapter, CCDs can be used as photodetectors in analogue equipment such as camcorders and video cameras. Digital and video CCD cameras differ in the way the photoelectron signal is processed and displayed. In digital systems, quanta of photoelectrons stored in the pixels are sent as an analogue voltage signal over a short distance to an analogue-to-digital converter (ADC) that changes the signal into the binary code of the computer. The converter is contained in the camera head, or in the camera control unit, or on a card in the computer. In video cameras there is no digitization step, and the signal remains in analogue format as a variable voltage signal. Video cameras also add synchronization pulses to the signal to generate the composite video signal required by the raster scanning mechanism in the TV monitor. Because a video CCD imager is read at a faster rate (30 frames/s or greater), read noise is higher, causing the dynamic range and S/N of a video image to be lower than in images produced by a slow-scan digital CCD camera. Finally, video signals are commonly recorded on a VCR tape, while digital images are usually stored as image files on the hard drive of a computer. Sometimes the distinction between digital and video cameras becomes blurred, since some CCD cameras contain dual video and digital output, and because video and digital signals can be easily interconverted.

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